Synthesis and Spectro Scopic Study of Some Metal Transition Amino Organic Compounds with N-(2-OXO-1,2-Dihydropyrimidin-4-Ylcarbamothioyl) Acetamide (DPA)

Authors

  • Thuraya A. Kader, Basima M. Sarhan

DOI:

https://doi.org/10.53350/pjmhs22166543

Keywords:

Cytosine, acetyl chloride, transition metals.

Abstract

A New ligand, N-(2-oxo-1,2- Dihydropyrimidin-4- ylcarbamothioyl) Acetamide (DPA) was prepared by reaction of iso thiosyanate derivative with Cytosine. The ligand has been characterized through elemental analysis, H1 NMR, C13NMR, FT-IR, and UV Visible spectra, such ligand’s transition metal complexes have been characterized through conductivity measurement, FT-IR, UV Visible spectra and magnetic susceptibility, all the complexes of this ligand are solid crystal  and molar ratio (2:1) (ligand: metal). The form of molecular for these complexes octa hedral. The general formula [M(DPA)2Cl2], where M+2 = (Mn, Co, Ni, Cu, Zn, Cd, Hg).

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How to Cite

Thuraya A. Kader, Basima M. Sarhan. (2022). Synthesis and Spectro Scopic Study of Some Metal Transition Amino Organic Compounds with N-(2-OXO-1,2-Dihydropyrimidin-4-Ylcarbamothioyl) Acetamide (DPA). Pakistan Journal of Medical & Health Sciences, 16(06), 543. https://doi.org/10.53350/pjmhs22166543